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NMR-Erfahrung

Ich biete langjährige Erfahrung auf folgenden Gebieten:

  • NMR in Lösung und im Festkörper, Bio-NMR, Semi-Festkörper/Polymere ("HR-MAS")
  • Agilent/Varian Software und Hardware
  • Training, Ausbildung, Kurse
  • Vorträge, Veröffentlichungen, Manuals
  • Strukturbestimmung und -verifizierung organischer Moleküle
  • Quantifizierung (QNMR), Reinheitsbestimmung
  • Diffusion ("DOSY")
  • Pulssequenz- (C) Makro- (MAGICAL) und Interface-Programmierung (XML)
  • GMP, CFR part 11 Setup (VnmrJ for Secure Environments)
  • Unix/Linux Systemadministration, Shell-Skripte, Backup

  • Publikationsliste:

    1. Craig P. Butts, Bert Heise and Godiarone Tatolo.
      SelEXSIDE: Fast and Easy Measurement of Multiple-Bond 1H,13C Coupling Constants for Stereochemical Analysis.
      Org. Lett. 14 (2012), 3256-3259.

    2. Jörg Leppert, Bert Heise, Oliver Ohlenschläger, Matthias Görlach and Ramadurai Ramachandran.
      Triple resonance MAS NMR with (13C, 15N) labelled molecules: reduced dimensionality data acquisition via 13C-15N heteronuclear two-spin coherence transfer pathways.
      Journal of Biomolecular NMR 28 (2004), 185-190.

    3. Jörg Leppert, Bert Heise, Oliver Ohlenschläger, Matthias Görlach and Ramadurai Ramachandran.
      Broadband RFDR with adiabatic inversion pulses.
      Journal of Biomolecular NMR 26 (2003), 13-24.

    4. Malgorzata Palczewska, Patrick Groves, Gyula Batta, Bert Heise and Jacek Kuznicki.
      Calretinin and calbindin D28k have different domain organizations.
      Protein Science 12 (2003), 180-184.

    5. Bert Heise, Jörg Leppert, Oliver Ohlenschläger, Matthias Görlach and Ramadurai Ramachandran.
      Chemical shift correlation via RFDR: Elimination of resonance offset effects.
      Journal of Biomolecular NMR 24 (2002), 237-243.

    6. Jörg Leppert, Bert Heise, Matthias Görlach and Ramadurai Ramachandran.
      REDOR: An assessment of the efficacy of dipolar recoupling with adiabatic inversion pulses.
      Journal of Biomolecular NMR 23 (2002), 227-238.

    7. Jörg Leppert, Bert Heise and Ramadurai Ramachandran.
      Orientational information from TEDOR spectral sidebands.
      Solid State Nuclear Magnetic Resonance 19 (2001), 1-18.

    8. Bert Heise, Jörg Leppert, Holger Wenschuh, Oliver Ohlenschläger, Matthias Görlach and Ramadurai Ramachandran.
      2D relayed anisotropy correlation NMR: Characterization of the 13C chemical shift tensor orientation in the peptide plane of the dipeptide AibAib.
      Journal of Biomolecular NMR 19 (2001), 167-179.

    9. Jörg Leppert, Bert Heise and Ramadurai Ramachandran.
      REDOR in IS1S2 systems.
      Journal of Biomolecular NMR 18 (2000), 153-164.

    10. Bert Heise, Jörg Leppert and Ramadurai Ramachandran.
      REDOR with adiabatic dephasing pulses.
      Journal of Magnetic Resonance 146 (2000), 181-187.

    11. Jörg Leppert, Bert Heise and Ramadurai Ramachandran.
      15N chemical shift tensor magnitude and orientation in the molecular frame of uracil determined via MAS NMR.
      Journal of Magnetic Resonance 145 (2000), 307-314.

    12. Bert Heise, Jörg Leppert and Ramadurai Ramachandran.
      Characterization of 15N chemical shift tensors via 15N-13C REDOR and 15N-1H dipolar shift CPMAS NMR spectroscopy.
      Solid State Nuclear Magnetic Resonance 16/3 (2000), 177-187.

    13. Roswitha Anders, Oliver Ohlenschläger, Vukic Šoškic, Holger Wenschuh, Bert Heise and Larry R. Brown.
      The NMR solution structure of the ion channel peptaibol chrysospermin C bound to dodecylphosphocholine micelles.
      European Journal of Biochemistry 267(6) (2000), 1784-1794.

    14. Jörg Leppert, Bert Heise and Ramadurai Ramachandran.
      Magic angle spinning NMR spectroscopy with composite RF pulses.
      Journal of Magnetic Resonance 139 (1999), 382-388.

    Doktorarbeit:

    Am Fritz Lipmann Institut für Altersforschung (FLI, vormals Institut für Molekulare Biotechnologie, IMB), Jena

    "NMR-Spektroskopie an Peptaibolen im Festkörper und in Lösung: Chemische Verschiebungstensoren in α-Aminoisobuttersäure und Strukturuntersuchungen an Chrysospermin C". PDF-Text (deutsch)